Insights on Morphology and Thermal Stability of Hollow Pt Nanospheres by In Situ Environmental TEM

Publication Alert with Atmosphere AX in Molecules for Heterogeneous Catalysis

Tuesday publication update! ๐Ÿ“– Have you ever wanted to see how nanomaterials behave under extreme conditions? Josephine Rezkallah, Xavier Sauvage, Bernhard Witulski and Simona Moldovan from the #UniversiteeRouenNormandie used the #AtmosphereAX system to investigated the real-time thermal evolution of hollow Pt nanospheres (HNSs) in both vacuum and 1 bar in situ hydrogen environments.

What did the authors observe?
๐Ÿ”ฅ They captured dynamic structural changes of Pt HNSs under heating
๐Ÿ”ฌ Observed shell formation and eventual collapse at temperatures >500ยฐC
๐Ÿ“ˆ Unraveled nanoparticle faceting, diffusion, and microstructural transformations
โš›๏ธ Provided 3D insights using electron tomography (ET) to map complex shell architectures

By visualizing nanomaterial behavior at atomic resolution, it is possible to get more insight into catalytic particle behavior, and therefore create more effective catalysts for future applications!

Want to read the entire paper? Find it here!
https://www.mdpi.com/1420-3049/30/4/792

2025 02 06 Atmosphere

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